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Trial synthesis
The best support will be provided for customer’s trial synthesis based on high temperature and high pressure technology.

Support for various trial test

Trial test, comissional test and joint reserch are provided based on supercritical water, hydrothermal synthesis and supercritical CO2 etc..
We offer the knowledge and know-how accumulated based on high temperature / high pressure technology over 10 years.
Please feel free to contact us!

  1. Flow type trial test for supercritical hydrothermal synthesis, hydrothermal synthesis, and solvothermal synthesis.
  2. Trial test using supercritical CO2.
  3. Drysnow cleaning test

1. Flow type trial test for supercritical hydrothermal synthesis, hydrothermal synthesis, and solvothermal synthesis.(Technical dataProduct information

Test condition for flow type trial test
Type of test Flow type nano particle synthesis, surface modification and material processing by using Momicho series.
Device Momicho miniMomicho mega(selected based on amount to be processed)
Option High pressure slurry pump
Washing and separation of the collected product
*Reaction kit (Purchase of reaction kit is recommended in order to avoid contamination)
Items to be prepared by customer Vessel to collect the product sample (about 1 L size)
Vessel for waste fluid (10L or 20L polyethylene tank)
Reagent or raw material to be processed
*If requested, all material can be prepared by ITEC

Operation of the system will be carried out by ITEC operator. Minimum will be from one day.

Test examples have been carried out
Nano particle, nano particle synthesis Zinc oxide (ZnO), Titanium oxide (TIO2), zirconium dioxide (ZrO2), barium titanate (TiBaO3), indium tin oxide (ITO), metallic nickel, silver (Ag), copper (Cu), ferrite system(M-Fe2O3), phosphor particles(Y2O3:Eu)
Surface modification particles Inorganic filler, (alumina (Al2O3, boron nitride, aluminum nitride (AlN), zinc oxide (ZnO), silica SiO2, carbon‐based material (C)) and organic modifications on above mentioned particles or other particles
Others Material, using supercritical water or subcritical water. Slurry processing (decomposition, dissolution and reaction)
The example of a test particle
(Synthesized by ITEC)
酸化亜鉛ナノ粒子
Zinc oxide nano particle
チタニアナノ粒子
Titania nano particle
有機修飾ジルコニアナノ粒子
Organically modified zirconia nano particle
有機修飾セリアナノ粒子
Organically modified seria nano particle
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2. Trial test using supercritical CO2(Product information

Supercritical CO2 test is provided for extraction, drying, concentration, dispersion, composition and surface modification.
Condition of trial CO2 test
Type of test Flow type test for CO2 processing, such as drying, concentration and extraction, for the samples.
Device Supercritical CO2 reaction lab testing machine
Items to be prepared by customer

Vessel to collect the product sample (about 1 L size)
*If requested, all material can be prepared by ITEC

Test examples have been carried out

Dispersion of carbon material, concentration of nano particle dispersion fluid and CO2 dissolution extraction.

 

 

3. Drysnow cleaning test(technical dataproduct information)

Try to see what it is like. Try to clean the samples.
Rental available.
Test condition for drysnow trial cleaning
Test condition Surface treatment or trial cleaning by Drysnow.
Test device Drysnow
Items to be prepared by customer Test samples
Test samples have been carried out Cleaning of print circuit board